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dc.contributor.authorBastos, Lívia Pinto Heckert
dc.date.accessioned2023-12-21T18:37:16Z-
dc.date.available2023-12-21T18:37:16Z-
dc.date.issued2019-09-10
dc.identifier.citationBASTOS, Lívia Pinto Heckert. Encapsulação do óleo essencial de pimenta preta (Piper nigrum L.) por coacervação complexa, utilizando proteínas e alginato de sódio como materiais de parede. 2019. 178 f]. Tese (Doutorado em Ciência e Tecnologia de Alimentos) - Instituto de Tecnologia, Universidade Federal Rural do Rio de Janeiro, Seropédica, 2019.por
dc.identifier.urihttps://rima.ufrrj.br/jspui/handle/20.500.14407/9303-
dc.description.abstractO óleo essencial (OE) de pimenta preta (Piper nigrum L.) é rico em compostos ativos como os terpenos, sendo sua aplicação como aditivo alimentar alvo de pesquisas, devido as suas atividades antimicrobianas e antioxidantes. Os terpenos, entretanto, são voláteis e quando expostos a certas condições (oxigênio, altas temperaturas, luz, baixos pHs, fluidos gastrointestinais) podem ter o seu potencial biológico reduzido e, nesse sentido, a microencapsulação é uma alternativa na proteção dos OE e seus componentes. Dentre os métodos de microencapsulação, a coacervação complexa apresenta vantagens como baixa concentração de materiais de parede, elevada eficiência de encapsulação, e uma variedade de biopolímeros que podem ser utilizados como materiais de parede. O objetivo deste trabalho foi caracterizar e avaliar a estabilidade do OE de pimenta preta (Piper nigrum L.) e de suas cápsulas formadas por diferentes biopolímeros pela técnica de coacervação complexa.Os biopolímeros e agentes reticulantes utilizados foram eficazes na proteção do OE apresentando elevada eficiência de encapsulação, preservando os principais terpenos no OE encapsulado. Adicionalmente, as cápsulas fabricadas com lactoferrina/alginato de sódio e β-lactoglobulina/alginato de sódio preservaram o OE quando expostos a condição oral e gástrica simuladas in vitro. Nas cápsulas produzidas pelo sistema β-lactoglobulina/alginato de sódio foi avaliada a liberação do óleo essencial em diferentes matrizes alimentícias simuladas, em matrizes alimentícias aquosas, ocorreu baixa liberação do OE, e sua liberação foi por difusão Fickian de acordo com modelo Rigger-Peppas. Os resultados obtidos sugerem que os materiais de parede utilizados foram eficientes e podem ser utilizados para encapsular novos ingredientes ativos.por
dc.description.sponsorshipCAPES - Coordenação de Aperfeiçoamento de Pessoal de Nível Superiorpor
dc.formatapplication/pdf*
dc.languageporpor
dc.publisherUniversidade Federal Rural do Rio de Janeiropor
dc.rightsAcesso Abertopor
dc.subjectbiopolímerospor
dc.subjectproteínas do soro do leitepor
dc.subjectinteração eletrostáticapor
dc.subjectterpenospor
dc.subjecteficiência de encapsulaçãopor
dc.subjectestabilidade térmicapor
dc.subjectbiopolymerseng
dc.subjectwhey proteinseng
dc.subjectelectrostatic interactioneng
dc.subjectterpeneseng
dc.subjectencapsulation efficiencyeng
dc.subjectthermal stabilityeng
dc.titleEncapsulação do óleo essencial de pimenta preta (Piper nigrum L.) por coacervação complexa, utilizando proteínas e alginato de sódio como materiais de paredepor
dc.title.alternativeEncapsulation of the black pepper (Piper nigrum L.) essential oil by complex coacervation using proteins and sodium alginate as wall materialseng
dc.typeTesepor
dc.description.abstractOtherThe black pepper (Piper nigrum L.) essential oil (EO) is a rich source of biologically active compounds (e.g.terpenes) and your applicability as a food additive has been the subject of several studies due to the antimicrobial and antioxidant activity of these compounds. Terpenes, however, are volatile and when exposed to certain conditions (high temperatures, light, low pH and gastrointestinal fluids) can reduce their biological potential and, in this sense, microencapsulation is an alternative way to the conserve EOs properties and their components. Among the microencapsulation methods, the complex coacervation method has advantages such as low concentrations of the wall materials, high encapsulation efficiency, and a variety of biopolymers that can be applied as wall materials. The aim of the present study was to characterize and evaluate the stability of black pepper EO encapsulated by complex coacervation using different biopolymers wall materials. The biopolymers and cross-linking agents used were effective in the protection of the EO, presented high encapsulation efficiency and preserved their main terpenes. Capsules formed by lactoferrin/sodium alginate and β-lactoglobulin/sodium alginate preserved the EO when exposed to simulated oral and gastric conditions in vitro. In simulated aqueous foods, the EO release was lower from β-lactoglobulin/sodium alginate microcapsules, and the EO release was by Fickian diffusion according to the Rigger-Peppas model. The obtained results suggest that the wall materials used were efficient and could be applied to encapsulate new active ingredients.eng
dc.contributor.advisor1Rojas, Edwin Elard Garcia
dc.contributor.advisor1IDCPF: 014.548.996-54por
dc.contributor.referee1Finotelli, Priscilla Vanessa
dc.contributor.referee2Sabino, Silvio José
dc.contributor.referee3Machado, Mariana Teixeira da Costa
dc.contributor.referee4Vicente, Juarez
dc.creator.IDCPF: 122.476.067-09por
dc.creator.Latteshttp://lattes.cnpq.br/1578379346432268por
dc.publisher.countryBrasilpor
dc.publisher.departmentInstituto de Tecnologiapor
dc.publisher.initialsUFRRJpor
dc.publisher.programPrograma de Pós-Graduação em Ciência e Tecnologia de Alimentospor
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dc.subject.cnpqCiência e Tecnologia de Alimentospor
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dc.originais.urihttps://tede.ufrrj.br/jspui/handle/jspui/5319
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